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<http://eprints.uny.ac.id/id/eprint/3603> <http://purl.org/dc/terms/title> "IMPREGNASI “TITANIUM OKSIDA” PADA MATERIAL SILIKAT MESOPORI-MESOSTRUKTUR MCM-41 "^^<http://www.w3.org/2001/XMLSchema#string> .
<http://eprints.uny.ac.id/id/eprint/3603> <http://purl.org/ontology/bibo/abstract> "Tujuan penelitian ini adalah uptuk mengimpregnasikan \"titanium oksida\" pada material silikat mesopori-mesostruktur MCM-41 clan mempelajari pengaruh konsentrasi prekursor [Ti8O,2(H'O)24]C1s.HC1. 7H,0 terhadap bentuk impregnasi \"titanium oksida\" dalam material silikat mesopori MCM-41. Silikat mesopori MCM-41 disintesis dengan menggunakan metode hidrotermal dengan tekanan autogenik pada temperatur 120` C selama 5, liar]. Kemudian padatan dikalsinasi 'pada temperatur 550° C selama 4 jam. Impre;~nasi material dilakukan dengan metode basah. Prekursor [TiQO,2(H~O),a]CI,.HCI_ 7H,0 (0; 25; 50; 75 clan 100 mg) dilarutkan ke dalam 30 mL larutan etanol absolut, kemudian ditambah 100 mg MCM-41. Larutan impregnan dipanaskan pada temperatur 60\" C dengan pengadukan 200 rpm dibawah aliran gas nitrogen selama 4 jam. Material yang terbentuk dikarakterisasi dengan FTIR_ XRD_ analisis kualitatif HNO-, pekat dan H2O2. Hasil karakterisasi menunjukkan bahwa metode impregnasi basah dapat digunakan untuk mempreparasi \"titanium oksida\" teremban material silikat tnesopori-mesostruktur MCM-41. \"Titanium oksida\" yang terimpregnasi pada permukaan MCM-41 melalui ikatan Ti-O-S] bertambahJ seiring dengan kenaikan konsentrasi prekursor saat impregnasi. \"Titanium oksida'\" yang paling banvak teremban di permukaan MCM-=11 yaitu pada rasio berat prekursor l MCM-41 - 1. "^^<http://www.w3.org/2001/XMLSchema#string> .
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