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<http://eprints.uny.ac.id/id/eprint/16978> <http://purl.org/dc/terms/title> "PENGARUH VARIASI RASIO MOL SINAMALDEHIDA-ASETON PADA SINTESIS 6-FENIL-3,5-HEKSADIEN-2-ON MENGGUNAKAN \r\nMETODE MAOS (Microwave Assist Organic Synthesis"^^<http://www.w3.org/2001/XMLSchema#string> .
<http://eprints.uny.ac.id/id/eprint/16978> <http://purl.org/ontology/bibo/abstract> "Penelitian ini bertujuan untuk mensintesis senyawa sinamalaseton dari senyawa sinamaldehida dan aseton menggunakan katalis NaOH melalui metode MAOS, mengetahui pengaruh variasi rasio mol sinamaldehida-aseton pada sintesis senyawa sinamalaseton yang dihasilkan, dan menentukan rasio mol sinamaldehida-aseton yang memberikan hasil rendemen maksimal.\r\nSintesis senyawa sinamalaseton dilakukan melalui reaksi kondensasi aldol silang dalam suasana basa antara sinamaldehida dan aseton dengan rasio mol 1:1, 1:5, 1:10, 1:15, dan 1:20. Alat yang digunakan dalam metode MAOS ini adalah microwave tipe SIGMATIC SMO-25SSG dengan waktu reaksi 120 detik. Produk hasil sintesis diidentifikasi menggunakan KLT, KLT scanner, FTIR dan 1H-NMR.\r\nSintesis senyawa sinamalaseton menggunakan metode MAOS dibutuhkan  waktu 120 detik. Variasi rasio mol sinamaldehida-aseton 1:1, 1:5, 1:10, 1:15, dan 1:20, menghasilkan rendemen sinamalaseton berturut-turut yaitu 7,269%; 29,810%; 54,530%; 22,443%; dan 9,411%. Rasio mol sinamaldehida-aseton (1:10) memiliki kemurnian 87,82% dan memberikan hasil rendemen maksimal yaitu 54,530%.\r\n\r\nKata kunci: kondensasi aldol silang, MAOS, sinamalaseton"^^<http://www.w3.org/2001/XMLSchema#string> .
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