TY  - JOUR
ID  - UNY11426
A1  - Djefry, Tani
A1  - Bambang, Setiaji
A1  - Wega, Trisunaryanti
A1  - Akhmad, Syoufian
TI  - EFFECT ACTIVATION OF CHEMICAL AND PHYSICAL TO STRUCTURE
AND ACTIVATED CARBON QUALITY FROM CHARCOAL OBTAINED BY
PYROLYSIS OF COCONUT SHELL
PB  - Yogyakarta State University
Y1  - 2014/05//
UR  - http://fmipa.uny.ac.id
KW  - coconut shell
KW  -  activated carbon 
KW  -  ZnCl2 
KW  -  SPSS 
KW  -  FTIR 
KW  -  SEM 
KW  -  BET
N2  - Activation of coconut shell charcoal has been done by a combination of chemical
and physical activation to determine the effect of chemical activators and activation
temperature to changes in the chemical structure and the quality of activated carbon .
The study was conducted on charcoal coconut shell of pyrolysis results with variation of
concentration and immersion time ZnCl2 as an activator , respectively 0.5 to 2 M for 12
to 24 hours . Then proceed with the activation of physics in reactor the activation of the
temperature variation of 500 to 800 oC with CO2 gas flow rate 20 mL / min . Evaluation
of the chemical structure and the quality of activated carbon performed FTIR , SEM ,
specific surface area , total pore volume , and average pore with Brunauer - Emmett -
Teller ( BET ) . The results showed the results of the analysis of SPSS through
Cofficients test the concentration variables most affect to moisture content , ash content ,
and iodine absorption from temperature variable and time of activation . The best quality
activated carbon produced at a concentration of ZnCl2 of 1.5 M, 24 hours soaking time of
24 hours , temperature 800 oC and the activation time of 120 minutes . The results as
moisture content of 8.47 % , volatile matter content of 18.55 % , ash content 1.44 % ,
bonded carbon content of 80.01 % and iodine absorption of 769.74 mg / g . The results
of FTIR analysis showed the surface of activated carbon containing CO and CH bonds ,
and SEM analysis showed the number and diameter of pores increased with the higher
calcination temperature . Surface area ( BET ) of 359.286 m2 / g , pore volume of 1.984 x
10-1 cm3 / g and pore mean of 11.46 ? .
AV  - public
JF  - Proceeding of International Conference On Research, Implementation And Education Of Mathematics And Sciences 2014
ER  -